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Survey of lip care products with fragrance and flavour

Appendix 2. Analytical results

Table 1 The results of the analysis for methyl eugenol. The results are given in mg/kg.

  53 80 93
A B A B A B
Methyl eugenol < 10 < 10 12 12 36 36

<: means less than the stated limit of detection

Table 2. The results from the analysis for fragrances. Unit is mg/kg. The two results indicate double determination.

  LOD 7 10 20 32 33
A B A B A B A B A B
Anisyl alcohol 1 - - - - - - - - - -
Amyl cinnamal 1 - - - - - - - - - -
Amylcinnamyl alcohol 1 - - - - - - - - - -
Benzyl alcohol 1 - - - - 30 33 - - 9 10
Benzyl benzoate 1 8 16 - - - - 110 96 - -
Benzylcinnamat 1 - - - - - - - - - -
Benzyl salicylat 1 - - - - - - - - - -
Cinnamyl alcohol 1 - - - - - - - - - -
Cinnamal 1 - - - - - - - - - -
Citral 1 1300 1100 - - - - 33 32 - -
Citronellol 1 - - - - - - - - - -
Coumarin 1 - - - - - - - - - -
Eugenol 1 - - - - - - - - - -
Farnesol 1 - - - - - - - - - -
Geraniol 1 9 11 - - - - 6 6 3 3
Hexylcinnamaldehyd 1 - - - - - - - - - -
Hydroxycitronellal 1 - - - - - - - - - -
α-Isomethylionon 1 66 71 - - - - - - - -
Lillial 1 - - - - - - - - - -
D-limonen 1 24000 21000 140 140 4 2 420 420 73 73
Linalool 1 880 810 - - - - 98 100 23 25
Lyral 1 - - - - - - - - - -
Isoeugenol 1 150 140 - - - - - - - -
Methyl heptin carbonat 1 - - - - - - - - - -
Oakmoss 10 - - - - - - - - - -
Treemoss 10 - - - - - - - - - -
Sum   26000 23000 140 140 34 35 670 650 110 110

LOD: means limit of detection
-: means not detected above the LOD

Table 2 continued. The results of the analysis for fragrances. Unit is mg/kg. The two results indicate double determination.

  LOD 35 37 45 51 53
A B A B A B A B A B
Anisyl alcohol 1 - - - - - - - - - -
Amyl cinnamal 1 - - - - - - - - - -
Amylcinnamyl alcohol 1 - - - - - - - - - -
Benzyl alcohol 1 - - 10 12 8 8 - - 6 4
Benzyl benzoate 1 - - - - 7 6 100 130 - -
Benzylcinnamate 1 - - - - 3 3 6 5 - -
Benzyl salicylate 1 - - - - 6 6 - - - -
Cinnamyl alcohol 1 - - - - - - - - - -
Cinnamal 1 - - - - - - - - - -
Citral 1 - - - - - - - - 57 55
Citronellol 1 56 52 - - - - 5 4 - -
Coumarin 1 - - - - - - - - - -
Eugenol 1 - - - - 16 14 41 40 - -
Farnesol 1 - - - - - - - - - -
Geraniol 1 180 190 - - - - - - 4 4
Hexylcinnamaldehyde 1 - - - - - - - - - -
Hydroxycitronellal 1 - - - - - - - - - -
α-Isomethylionon 1 - - - - - - - - - -
Lillial 1 - - - - - - - - - -
D-limonene 1 76 74 3 4 460 470 9 9 16000 15000
Linalool 1 19 19 - - 150 160 - - 24 26
Lyral 1 - - - - - - - - - -
Isoeugenol 1 - - - - - - 3 3 - -
Methyl heptine carbonate 1 - - - - - - - - - -
Oakmoss 10 - - - - - - - - - -
Treemoss 10 - - - - - - - - - -
Sum   330 330 13 16 650 670 160 190 16000 15000

LOD: means limit of detection
-: means not detected above the LOD

Table 2 continued. The results of the analysis for fragrances. Unit is mg/kg. The two results indicate double determination.

  LOD 57 66 75 80 86
A B A B A B A B A B
Anisyl alcohol 1 - - - - - - - - - -
Amyl cinnamal 1 - - - - - - - - - -
Amylcinnamyl alcohol 1 - - - - - - - - - -
Benzyl alcohol 1 - - 23 24 - - 14 15 - -
Benzyl benzoate 1 7200 7000 6700 6600 - - 14 12 - -
Benzylcinnamate 1 - - - - - - 8 6 - -
Benzyl salicylate 1 - - - - - - - - - -
Cinnamyl alcohol 1 - - - - - - 6 7 - -
Cinnamal 1 - - - - - - - - - -
Citral 1 24 22 - - - - - - - -
Citronellol 1 - - - - 760 730 220 220 - -
Coumarine 1 - - - - - - - - - -
Eugenol 1 - - - - 86 87 46 46 - -
Farnesol 1 - - - - - - 5 6 - -
Geraniol 1 - - - - 720 730 98 96 - -
Hexylcinnamaldehyde 1 - - - - - - - - - -
Hydroxycitronellal 1 - - - - - - - - - -
α-Isomethylionon 1 - - - - - - - - - -
Lillial 1 - - - - - - - - - -
D-limonene 1 4 3 12 11 170 170 6 6 - -
Linalool 1 70 69 - - 800 770 5 5 - -
Lyral 1 - - - - - - - - - -
Isoeugenol 1 - - - - - - - - - -
Methyl heptine carbonaet 1 - - - - - - - - - -
Oakmoss 10 - - - - - - - - - -
Treemoss 10 - - - - - - - - - -
Sum   7300 7100 6700 6600 2500 2500 420 420 - -

LOD: means limit of detection
-: means not detected above the LOD

Table 2 continued. The results of the analysis for fragrances. Unit is mg/kg. The two results indicate double determination.

  LOD 91 93 94 97 106
A B A B A B A B A B
Anisyl alcohol 1 - - - - - - - - - -
Amyl cinnamal 1 - - - - - - - - - -
Amylcinnamyl alcohol 1 - - - - - - - - - -
Benzyl alcohol 1 - - 8 10 1800 1800 27 29 - -
Benzyl benzoate 1 - - 7 6 - - - - - -
Benzylcinnamate 1 - - - - - - - - - -
Benzyl salicylate 1 - - - - - - - - - -
Cinnamyl alcohol 1 - - - - - - - - - -
Cinnamal 1 - - 2 1 - - - - - -
Citral 1 - - - - - - - - - -
Citronellol 1 - - 410 410 - - - - - -
Coumarine 1 - - - - - - - - 6 5
Eugenol 1 - - 29 24 22 21 - - - -
Farnesol 1 - - 11 10 - - - - - -
Geraniol 1 - - 140 140 - - - - - -
Hexylcinnamaldehyde 1 - - - - - - - - - -
Hydroxycitronellal 1 - - - - - - - - - -
α-Isomethylionon 1 - - - - - - - - - -
Lillial 1 - - - - - - - - - -
D-limonene 1 6 6 770 790 3 3 2600 2600 20 20
Linalool 1 - - 31 28 97 94 42 39 - -
Lyral 1 - - - - - - - - - -
Isoeugenol 1 - - - - - - - - - -
Methyl heptine carbonate 1 - - - - - - - - - -
Oakmoss 10 - - - - - - - - - -
Treemoss 10 - - - - - - - - - -
Sum   6 6 1400 1400 1900 1900 2700 2700 26 25

LOD: means limit of detection
-: means not detected above the LOD

 

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Version 1.0 March 2006, © Danish Environmental Protection Agency