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Survey and release of chemical substances in "slimy" toys
Enclosure D: GC-MS Analysis results from screening
Analysis results for sweat-extracts stated in µg/g sample
| ID no. DK-01, exterior |
Sample amount: 1.83 g |
| Chemical Technology label 30396-1 |
|
| Component |
CAS no. |
µg/g |
| Toluene |
108-88-3 |
0.25 |
| Naphthalene |
91-20-3 |
0.02 |
| Ethanol-2-(butoxy ethoxy)acetate |
112-15-2 |
0.2 |
Analysis results for saliva-extracts stated in µg/g sample
| ID no. DK-01, exterior |
Sample amount: 1.98 g |
| Chemical Technology label 30396-1 |
|
| Component |
CAS no. |
µg/g |
| Toluene |
108-88-3 |
0.31 |
| Naphthalene |
91-20-3 |
0.02 |
| Ethanol-2-(butoxy ethoxy)acetate |
112-15-2 |
0.2 |
Comments
The components were identified by comparing the respective mass spectra with mass spectra from NIST library.
The stated amounts are calculated according to response for internal standards assuming that all detected components have same response for same amount and same recovery.
Analysis results for sweat-extracts stated in µg/g sample
| ID no. DK-02, exterior |
Sample amount: 1.30 g |
| Chemical Technology label 30396-2 |
|
| Component |
CAS no. |
µg/g |
| Toluene |
108-88-3 |
0.10 |
Analysis results for saliva-extracts stated in µg/g sample
| ID no. DK-02, exterior |
Sample amount: 1.97 g |
| Chemical Technology label 30396-2 |
|
| Component |
CAS no. |
µg/g |
| Toluene |
108-88-3 |
0.09 |
Comments
The components were identified by comparing the respective mass spectra with mass spectra from NIST library.
The stated amounts are calculated according to response for internal standards assuming that all detected components have same response for same amount and same recovery.
Analysis results for sweat-extracts stated in µg/g sample
| ID no. DK-03, exterior |
Sample amount: 1.14 g |
| Chemical Technology label 30396-3 |
|
| Component |
CAS no. |
µg/g |
| Toluene |
108-88-3 |
0.15 |
| Cyclohexanone |
108-94-1 |
0.2 |
Analysis results for saliva-extracts stated in µg/g sample
| ID no. DK-03, exterior |
Sample amount: 1.17 g |
| Chemical Technology label 30396-3 |
|
| Component |
CAS no. |
µg/g |
| Toluene |
108-88-3 |
0.26 |
| Cyclohexanone |
108-94-1 |
0.2 |
Comments
The components were identified by comparing the respective mass spectra with mass spectra from NIST library.
The stated amounts are calculated according to response for internal standards assuming that all detected components have same response for same amount and same recovery.
Analysis results for sweat-extracts stated in µg/g sample
| ID no. K-01, exterior |
Sample amount: 2.34 g |
| Chemical Technology label 30396-5 |
|
| Component |
CAS no. |
µg/g |
| Toluene |
108-88-3 |
1.8 |
Analysis results for saliva-extracts stated in µg/g sample
| ID no. K-01, exterior |
Sample amount: 1.90 g |
| Chemical Technology label 30396-5 |
|
| Component |
CAS no. |
µg/g |
| Toluene |
108-88-3 |
1.9 |
Comments
The components were identified by comparing the respective mass spectra with mass spectra from NIST library.
The stated amounts are calculated according to response for internal standards assuming that all detected components have same response for same amount and same recovery.
Analysis results for sweat-extracts stated in µg/g sample
| ID no. K-01, gel |
Sample amount: 2.31 g |
| Chemical Technology label 30396-5 |
|
| Component |
CAS no. |
µg/g |
| Aliphatic hydrocarbon >C14 |
|
0.1 |
Analysis results for saliva-extracts stated in µg/g sample
| ID no. K-01, gel |
Sample amount: 1.57g |
| Chemical Technology label 30396-5 |
|
| Component |
CAS no. |
µg/g |
| Aliphatic hydrocarbon >C14 |
|
0.9 |
Comments
The components were identified by comparing the respective mass spectra with mass spectra from NIST library.
The stated amounts are calculated according to response for internal standards assuming that all detected components have same response for same amount and same recovery.
Analysis results for sweat-extracts stated in µg/g sample
| ID no. BR-01, exterior |
Sample amount: 2.39 g |
| Chemical Technology label 30396-7 |
|
| Component |
CAS no. |
µg/g |
| Toluene |
108-88-3 |
0.14 |
| o-, m, -p-Xylene, ethylbenzene |
95-47-5,108-38-3,
106-42-3, 100-41-4 |
2.3 |
Analysis results for saliva-extracts stated in µg/g sample
| ID no. BR-01, exterior |
Sample amount: 2.23 g |
| Chemical Technology label 30396-7 |
|
| Component |
CAS no. |
µg/g |
| Toluene |
108-88-3 |
0.17 |
| o-, m, -p-Xylene, ethylbenzene |
95-47-5,108-38-3,
106-42-3, 100-41-4 |
2.4 |
Comments
The components were identified by comparing the respective mass spectra with mass spectra from NIST library.
The stated amounts are calculated according to response for internal standards assuming that all detected components have same response for same amount and same recovery.
Analysis results for sweat-extracts stated in µg/g sample
| ID no. F-01, exterior |
Sample amount: 2.69 g |
| Chemical Technology label 30396-8A |
|
| Component |
CAS no. |
µg/g |
| Toluene |
108-88-3 |
0.16 |
| 3,5,5-Trimethyl-2-cyclohexen-1-one |
78-59-1 |
0.06 |
| 2-Phenoxy ethanol |
122-99-6 |
0.4 |
Analysis results for saliva-extracts stated in µg/g sample
| ID no. F-01, exterior |
Sample amount: 2.23 g |
| Chemical Technology label 30396-8A |
|
| Component |
CAS no. |
µg/g |
| Toluene |
108-88-3 |
0.21 |
| 3,5,5-Trimethyl-2-cyclohexen-1-one |
78-59-1 |
0.05 |
| 2-Phenoxy ethanol |
122-99-6 |
0.5 |
Comments
The components were identified by comparing the respective mass spectra with mass spectra from NIST library.
The stated amounts are calculated according to response for internal standards assuming that all detected components have same response for same amount and same recovery.
Analysis results for sweat-extracts stated in µg/g sample
| ID no. F-01, interior (yellow egg yolk) |
Sample amount: 3.37 g |
| Chemical Technology label 30396-8C |
|
| Component |
CAS no. |
µg/g |
| Toluene |
108-88-3 |
0.23 |
| 3,5,5-Trimethyl-2-cyclohexen-1-one |
78-59-1 |
0.05 |
| 2-Phenoxy ethanol |
122-99-6 |
0.5 |
Analysis results for saliva-extracts stated in µg/g sample
| ID no. F-01, interior (yellow egg yolk) |
Sample amount: 2.64 g |
| Chemical Technology label 30396-8C |
|
| Component |
CAS no. |
µg/g |
| Toluene |
108-88-3 |
0.29 |
| 3,5,5-Trimethyl-2-cyclohexen-1-one |
78-59-1 |
0.03 |
| 2-Phenoxy ethanol |
122-99-6 |
0.3 |
Comments
The components were identified by comparing the respective mass spectra with mass spectra from NIST library.
The stated amounts are calculated according to response for internal standards assuming that all detected components have same response for same amount and same recovery.
Analysis results for sweat-extracts stated in µg/g sample
| ID no. TO-01, exterior |
Sample amount: 2.16 g |
| Chemical Technology label 30396-9 |
|
| Component |
CAS no. |
µg/g |
| Cyclohexanone |
108-94-1 |
57 |
| Methyl parabene |
99-76-3 |
3.9 |
| 1,2-Propandion-1-phenyl-2-oxim |
119-51-7 |
5.8 |
| Propyl parabene |
94-13-3 |
5.3 |
| Benzoic acid-propylester |
2315-68-6 |
12 |
| Benzoic acid-butylester |
136-60-7 |
10 |
| Benzoic acid-phenylester |
93-99-2 |
0.3 |
| N-Propyl benzamide + N-acetyl benzamide |
10546-70-0 + 1575-95-7 |
2.4 |
| Diethylglycol dibenzoate etc. |
e.g. 120-55-8 |
127 |
| Diethylglycol dibenzoate etc. |
|
99 |
Analysis results for saliva-extracts stated in µg/g sample
| ID no. TO-01, exterior |
Sample amount: 2.41 g |
| Chemical Technology label 30396-9 |
|
| Component |
CAS no. |
µg/g |
| Cyclohexanone |
108-94-1 |
14 |
| Methyl parabene |
99-76-3 |
1.8 |
| 1,2-Propandion-1-phenyl-2-oxim |
119-51-7 |
3.0 |
| Propyl parabene |
94-13-3 |
3.3 |
| Benzoic acid-propylester |
2315-68-6 |
6.9 |
| Benzoic acid-butylester |
136-60-7 |
5.1 |
| Benzoic acid-phenylester |
93-99-2 |
0.2 |
| N-Propyl benzamide + N-acetyl benzamide |
10546-70-0 + 1575-95-7 |
36 |
| Diethylglycol dibenzoate etc. |
e.g. 120-55-8 |
115 |
| Diethylglycol dibenzoate etc. |
|
114 |
Comments
The components were identified by comparing the respective mass spectra with mass spectra from NIST library.
The stated amounts are calculated according to response for internal standards assuming that all detected components have same response for same amount and same recovery.
Analysis results for sweat-extracts stated in µg/g sample
| ID no. TO-02, exterior |
Sample amount: 2.31 g |
| Chemical Technology label 30396-10 |
|
| Component |
CAS no. |
µg/g |
| Cyclohexanone |
108-94-1 |
0.6 |
| Methyl parabene |
99-76-3 |
2.2 |
| 1,2-Propandion-1-phenyl-2-oxim |
119-51-7 |
0.2 |
| Propyl parabene |
94-13-3 |
1.9 |
| Benzoic acid-propylester (etc.) |
2315-68-6 |
0.8 |
| Benzoic acid-butylester (etc.) |
136-60-7 |
0.7 |
| Benzoic acid-phenylester (etc.) |
93-99-2 |
1.1 |
| N-Propyl benzamide + N-acetyl benzamide |
10546-70-0 + 1575-95-7 |
0.7 |
| Diethylglycol dibenzoate etc. |
e.g. 120-55-8 |
25 |
| Diethylglycol dibenzoate etc. |
|
4.1 |
Analysis results for saliva-extracts stated in µg/g sample
| ID no. TO-02, exterior |
Sample amount: 1.97 g |
| Chemical Technology label 30396-10 |
|
| Component |
CAS no. |
µg/g |
| Cyclohexanone |
108-94-1 |
0.2 |
| Methyl parabene |
99-76-3 |
0.6 |
| 1,2-Propandion-1-phenyl-2-oxim |
119-51-7 |
0.8 |
| Propyl parabene |
94-13-3 |
1.2 |
| Benzoic acid-propylester (etc.) |
2315-68-6 |
0.5 |
| Benzoic acid-butylester (etc.) |
136-60-7 |
0.4 |
| Benzoic acid-phenylester (etc.) |
93-99-2 |
0.2 |
| N-Propyl benzamide + N-acetyl benzamide |
10546-70-0 + 1575-95-7 |
1.6 |
| Diethylglycol dibenzoate etc. |
e.g. 120-55-8 |
16 |
| Diethylglycol dibenzoate etc. |
|
3.7 |
Comments
The components were identified by comparing the respective mass spectra with mass spectra from NIST library.
The stated amounts are calculated according to response for internal standards assuming that all detected components have same response for same amount and same recovery.
Analysis results for sweat-extracts stated in µg/g sample
| ID no. TO-03, gel |
Sample amount: 2.10 g |
| Chemical Technology label 30396-11 |
|
| Component |
CAS no. |
µg/g |
| 3,5,5-Trimethyl-2-cyclohexen-1-one |
78-59-1 |
0.3 |
| 2-Phenoxy ethanol |
122-99-6 |
145 |
| Methyl parabene |
99-76-3 |
1.6 |
| Ethyl parabene |
120-47-8 |
2.2 |
| Propyl parabene |
94-13-3 |
0.6 |
| Methyldihydrojasmonat |
24851-98-7 |
0.2 |
| Butyl parabene |
94-26-7 |
0.9 |
| Benzoic acid-propylester (etc.) |
2315-68-6 |
1.5 |
| 2-Phenylmethylenoctanal(= Hexylcinnamaldehyde)
Allergenic odorant
|
101-86-0 |
0.3 |
Analysis results for saliva-extracts stated in µg/g sample
| ID no. TO-03, lip-gloss |
Sample amount: 0.64 g |
| Chemical Technology label 30396-11 |
|
| Component |
CAS no. |
µg/g |
| 3,5,5-Trimethyl-2-cyclohexen-1-one |
78-59-1 |
1.4 |
| Propyl parabene |
94-13-3 |
23 |
| Component not identified |
|
12 |
| Component not identified |
|
5.8 |
| Component not identified |
|
4.2 |
| Component not identified |
|
4.2 |
| Component not identified |
|
5.2 |
Comments
The components were identified by comparing the respective mass spectra with mass spectra from NIST library.
The stated amounts are calculated according to response for internal standards assuming that all detected components have same response for same amount and same recovery.
Analysis results for sweat-extracts stated in µg/g sample
| ID no. G-01, exterior |
Sample amount: 2.98 g |
| Chemical Technology label 30396-12 |
|
| Component |
CAS no. |
µg/g |
| Toluene |
108-88-3 |
0.05 |
| o-, m, -p-Xylene, ethylbenzene |
95-47-5,108-38-3,
106-42-3, 100-41-4 |
0.1 |
| Cyclohexanone |
108-94-1 |
0.1 |
Analysis results for saliva-extracts stated in µg/g sample
| ID no. G-01, exterior |
Sample amount: 3.13 g |
| Chemical Technology label 30396-12 |
|
| Component |
CAS no. |
µg/g |
| Toluene |
108-88-3 |
Trace <0.05 |
| o-, m, -p-Xylene, ethylbenzene |
95-47-5,108-38-3,
106-42-3, 100-41-4 |
0.08 |
| Cyclohexanone |
108-94-1 |
Trace <0.05 |
Comments
The components were identified by comparing the respective mass spectra with mass spectra from NIST library.
The stated amounts are calculated according to response for internal standards assuming that all detected components have same response for same amount and same recovery.
Analysis results for sweat-extracts stated in µg/g sample
| ID no. K-03, exterior |
Sample amount: 2.26 g |
| Chemical Technology label 30396-13 |
|
| Component |
CAS no. |
|
| Toluene |
108-88-3 |
Trace <0.02 |
| Hydrocarbons > C14 |
|
2 |
Analysis results for saliva-extracts stated in µg/g sample
| ID no. K-03, exterior |
Sample amount: 1.96 g |
| Chemical Technology label 30396-13 |
|
| Component |
CAS no. |
µg/g |
| Toluene |
108-88-3 |
Trace <0.02 |
| Hydrocarbons > C14 |
|
3 |
Comments
The components were identified by comparing the respective mass spectra with mass spectra from NIST library.
The stated amounts are calculated according to response for internal standards assuming that all detected components have same response for same amount and same recovery.
Analysis results for sweat-extracts stated in µg/g sample
| ID no. TI-01, exterior |
Sample amount: 1.29 g |
| Chemical Technology label 30396-16 |
|
| Component |
CAS no. |
µg/g |
| Toluene |
108-88-3 |
Trace <0.05 |
| 3,5,5-Trimethyl-2-cyclohexen-1-one |
78-59-1 |
0.8 |
Analysis results for saliva-extracts stated in µg/g sample
| ID no. TI-01, exterior |
Sample amount: 1.35 g |
| Chemical Technology label 30396-16 |
|
| Component |
CAS no. |
µg/g |
| Toluene |
108-88-3 |
Trace <0.05 |
| 3,5,5-Trimethyl-2-cyclohexen-1-one |
78-59-1 |
0.7 |
Comments
The components were identified by comparing the respective mass spectra with mass spectra from NIST library.
The stated amounts are calculated according to response for internal standards assuming that all detected components have same response for same amount and same recovery.
Analysis results for sweat-extracts stated in µg/g sample
| ID no. R-01, exterior |
Sample amount: 2.67 g |
| Chemical Technology label 30396-17 |
|
| Component |
CAS no. |
µg/g |
| 5-Methyl-2-(1-methylethylcyclohexanol) |
23283-97-8 |
0.1 |
| 2-Phenoxy ethanol |
122-99-3 |
1.8 |
Analysis results for saliva-extracts stated in µg/g sample
| ID no. R-01, exterior |
Sample amount: 1.84 g |
| Chemical Technology label 30396-17 |
|
| Component |
CAS no. |
µg/g |
| 5-Methyl-2-(1-methylethylcyclohexanol) |
23283-97-8 |
0.2 |
| 2-Phenoxy ethanol |
122-99-3 |
1.6 |
Comments
The components were identified by comparing the respective mass spectra with mass spectra from NIST library.
The stated amounts are calculated according to response for internal standards assuming that all detected components have same response for same amount and same recovery.
Analysis results for sweat-extracts stated in µg/g sample
| ID no. A-01, exterior |
Sample amount: 2.02 g |
| Chemical Technology label 30396-18 |
|
| Component |
CAS no. |
µg/g |
| Toluene |
108-88-3 |
Trace <0.05 |
| o-, m, -p-Xylene, ethylbenzene |
95-47-5,108-38-3,
106-42-3, 100-41-4 |
0.90 |
Analysis results for saliva-extracts stated in µg/g sample
| ID no. A-01, exterior |
Sample amount: 2.05 g |
| Chemical Technology label 30396-18 |
|
| Component |
CAS no. |
µg/g |
| Toluene |
108-88-3 |
Trace <0.05 |
| o-, m, -p-Xylene, ethylbenzene |
95-47-5,108-38-3,
106-42-3, 100-41-4 |
0.86 |
Comments
The components were identified by comparing the respective mass spectra with mass spectra from NIST library.
The stated amounts are calculated according to response for internal standards assuming that all detected components have same response for same amount and same recovery.
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Version 1.0 March 2006, © Danish Environmental Protection Agency
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